Thirunavukarasu, P. (1999) Electrosynthesis of 5-chloro diethyl,4 DICHLORO PHENOXY) benzanamine using titanous (fitanic redox mediator. Bulletin of Electrochemistry , 15 (7-8). pp. 280-282. ISSN 0256-1654

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Abstract

The titled compound is the precussor in the preparation of Triclosan [5-chloro-Z-(Z,4 Dichloro phenoxy) phenol], an important antihacterial, very much used in cosmetic fommlations, is nonllally obtained hy the chemical reduction of 4·chloro-l-(Z,4-dichloro phenoxy).Z-nitro benzene using metaVaciti or hy the catalytic hydrogenation using Raney Nickel catalyst. The synthesis of the titled compound is tried hy I ctrochemical route using. titanous/titanic redox couple. The effect of current density, temperatun' of the e1ectrolysi", the depolariser concentration and the type of the solvent used during the electrolysis are discussed in the pape.-.

Item Type:	Article
Uncontrolled Keywords:	Triclosan; redox couple and depolariser
Subjects:	Electroorganic
Divisions:	UNSPECIFIED
Depositing User:	ttbdar CECRI
Date Deposited:	21 Feb 2012 07:21
Last Modified:	21 Feb 2012 07:21
URI:	http://cecri.csircentral.net/id/eprint/1157

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