Thirunavukarasu, P.
(1999)
Electrosynthesis of 5-chloro diethyl,4 DICHLORO PHENOXY)
benzanamine using titanous (fitanic redox mediator.
Bulletin of Electrochemistry , 15 (7-8).
pp. 280-282.
ISSN 0256-1654
Abstract
The titled compound is the precussor in the preparation of Triclosan [5-chloro-Z-(Z,4 Dichloro phenoxy) phenol], an important antihacterial, very much used in cosmetic fommlations, is nonllally obtained hy the chemical reduction of 4·chloro-l-(Z,4-dichloro phenoxy).Z-nitro benzene using metaVaciti or hy the catalytic hydrogenation using Raney Nickel catalyst. The synthesis of the titled compound is tried hy I ctrochemical route using. titanous/titanic redox couple. The effect of current density, temperatun' of the e1ectrolysi", the depolariser concentration and the type of the solvent used during the electrolysis are
discussed in the pape.-.
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