Anbukulandainathan, M. and Kulangiappar, K. and Elangovan, M. and Raju, T. and Govindu, S.
(2000)
Synthesis of 2-chloro-p-xylene from p-xylene through two phase electrolysis.
Bulletin of Electrochemistry , 16 (9).
ISSN 0256-1654
Abstract
By employing a precious metal oxide coated over titanium as anode, electrolysis of p-xylene in an aqueous hydrochloric acid medium yielded a mixture of mono and dichloro-p-xyJene in the ratio of
3.5:1. A detailed investigation, employing various electrochemical parameters, resulted in a high yield of these products. These products were separated in 100% pure form and analysed through NMR and other common organic analysis. The products were found to be 20-chloro-p-xylene and 2,5-dichloro-p-xylene.
| Item Type: |
Article
|
| Uncontrolled Keywords: |
2-chloro and 2,S-dichloro-p-xylene; electrochemical preparation; temperature and mixing effect |
| Subjects: |
Electroorganic |
| Divisions: |
UNSPECIFIED |
| Depositing User: |
ttbdar CECRI
|
| Date Deposited: |
24 Feb 2012 17:38 |
| Last Modified: |
24 Feb 2012 17:38 |
| URI: |
http://cecri.csircentral.net/id/eprint/974 |
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