Berchmans, L.J. and Bharathi, B. and Amalajyothi, K. and Subramanian, K. (2009) Synthesis of Nanocrystalline Boron Nitride by Combustion Process. International Journal of Self-Propagating High-Temperature Synthesis, 18 (1). pp. 34-37.

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Abstract

Nanocrystalline boron nitride powders were synthesized by combustion process using urea as a fuel. Experiments were carried out by heating boric acid and urea in an N 2 atmosphere at 850 ° C. Boric acid was used as a source of boron while urea, as a source of nitrogen. The reactions were carried out in an autoclave with provisions for purging with nitrogen gas. The samples were characterized by powder X-ray diffraction, Fourier transform IR spectroscopy (FT-IR), FT-Raman spectroscopy, UV-VIS spectroscopy, and SEM.

Item Type: Article
Uncontrolled Keywords: combustion synthesis; hexagonal boron nitride; FT-IR; FT-Raman; UV-VIS spectroscopy; SEM
Subjects: Electropyrometallurgy
Divisions: UNSPECIFIED
Depositing User: TTBD CECRI
Date Deposited: 08 Apr 2012 14:56
Last Modified: 15 Jun 2012 07:52
URI: http://cecri.csircentral.net/id/eprint/369

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