Helan, M. and Berchmans, L.J. and Zahirhussain, A. (2010) Synthesis of LiMn2O4 by molten salt technique. Ionics, 16. pp. 227-231. ISSN 0947-7047

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Lithium manganese oxide powders have been successfully prepared by a molten salt synthesis using eutectic mixture of LiCl and MnO2 salt at 900 °C. The synthesis was performed in open atmosphere. The crystalline powders were characterized for their phase identification using X-ray diffraction analysis. The physicochemical properties of the lithium manganese oxide powders are investigated by thermal analysis (thermo gravimetric analysis/ differential thermal analysis), Fourier transform infrared spectroscopy, Raman spectroscopy, atomic absorption spectroscopy, electron spin resonance spectroscopy, and scanning electron microscopy. This work shows the feasibility for obtaining lithium manganese oxide at lowtemperature molten salt flux method.

Item Type: Article
Uncontrolled Keywords: LiMn2O4; Molten salt synthesis; Cathode materials; batteries; Cathodes; Li-ion batteries; Materials preparations
Subjects: Electropyrometallurgy
Lithium batteries
Depositing User: ttbdar CECRI
Date Deposited: 08 May 2012 08:39
Last Modified: 08 May 2012 08:39
URI: http://cecri.csircentral.net/id/eprint/268

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